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Lab notes - Purified Tea Tree Oil Experiments for Making Sodium

In this video we purify tea tree oil by fractional distillation to extra to 4-terpineol. 4-Terpineol turns out to be a reasonably good catalyst for the sodium production reaction. Related Videos: Using grignards to make tertiary alcohols: https://www.youtube.com/watch?v=EFQWD7-DCPI Previous lab notes on making sodium involving tea tree oil: https://www.youtube.com/watch?v=v7o3ZfX0BQc Donate to NurdRage! Through Patreon (preferred): https://www.patreon.com/NurdRage Through Bitcoin: 1NurdRAge7PNR4ULrbrpcYvc9RC4LDp9pS Glassware generously provided by http://www.alchemylabsupply.com/ Use the discount code "nurdrage" for a 5% discount. Twitter: https://twitter.com/NurdRage Reddit: https://www.reddit.com/r/NurdRage/ Facebook: https://www.facebook.com/NurdRageYoutube/ Instagram: https://www.instagram.com/nurdrageyoutube/ #sodium #4-Terpineol #TeaTreeOil

Comments

Anonymous

I was wondering if there is a way of recovering the magnesium oxide and turning it back to magnesium metal?

Twizzy

Would hydrating rather than hydrogenating be easier? It would give a dual tertiary alcohol which might make the precipitation problem worse though.

NurdRage

requires far too high a temperature. So i probably won't attempt it.

NurdRage

i actually did try it, but it didn't seem to work. Granted, i didn't try very hard, i figure if i need to put in MORE effort than distilling tea tree oil then it's not worth it. (as that effort is better spent just with tea tree oil.)

Jeff Evarts

This is awesome, keep turning the crank - we appreciate it. A nit: Are you still counting the alcohol as a catalyst if it is indeed consumed?

Anonymous

Would vacuum distillation allow you to use a full column and get better separation?

Anonymous

It isn't consumed by the sodium production reaction, it probably just decomposes in the presence of side products at elevated temperatures.

Anonymous

Looking forward to the hydrogenation reaction. I managed to get some palladium on carbon for cheap if you want I can send you a bottle.

Anonymous

Would Urushibara Nickel work?