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This is the second part! 


Let me know what you guys think of this project. If any of you guys think you have something that you can properly cure the novolac in, let me know! 

Files

Making Bakelite Plastic (Part 2)

NileRed store (Glassware & Beaker Mugs): https://nile.red/shop Link to part 1: https://www.youtube.com/edit?o=U&video_id=phNLecfyWS8 In part 2, I will be finishing things off and making the novolac. Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA -------------------------------- Patreon: https://www.patreon.com/nilered Youtube Membership: https://www.youtube.com/c/nilered/join NileRed Merch Store (NileRed Pin & Keychain): https://store.dftba.com/collections/nilered NileRed Website (Glassware & Beaker Mugs): https://nile.red -------------------------------- Instagram: https://www.instagram.com/nile.red Twitter: https://twitter.com/NileRed2 Discord: https://discord.gg/3BT6UHf

Comments

Gabriel J.

Could using a pressure cooker instead of a toaster oven help with the bubbling? Cool stuff otherwise. Where'd you get your phenol from?

Anonymous

Those cheap electronics prototyping boards (the tan ones with a gridwork of holes, and maybe pre-made copper traces) are made of phenol-formaldehyde resin bonded with paper. I can imagine putting the paper and melted bakelite through some sort of press or rollers. That might take care of any bubbles in the p-f resin and press it into the pores in the paper. The better boards, those used in real consumer electronics , are woven fiberglass in an epoxy matrix. How hard is it to make epoxy resins?

Anonymous

The process you explored in these videos is really interesting. I might have a go at this synthesis as it would be interesting to explore alternative curing methods in detail... all assuming I have the time available. Many thanks for an inspiring and entertaining video.

Silviu T

A pressure cooker won't get you too far. You can go up to about 3atm with it which probably won't do much to limit the bubbling. You need a small but strong pressure vessel, which you'd occupy a significant fraction of the interior volume of with the novolac or resol. This way the initial outgassing will serve to pressurize the vessel sufficiently to limit the subsequent bubbling. It would also need to be a slow process. Essentially reinventing the bakelizer. I have no idea what you could use off-the-shelf for this purpose, it'd need to be custom built I guess.

nilered

Very true. Thanks for the input. I am not sure I want to re-invent it, ha.

nilered

I'm glad you liked it. I wish you luck if you try it yourself!

nilered

I'm not sure. But I want to try to make as many commercial polymers as I can. So I'll look into epoxies