GordoTEK Organic Chemistry Extraction with FAQ (Revised 2019 edition, BEST methods)
If you'd like to support GordoTEK or request a topic, please use patreon, I also post and interact with people there: https://www.patreon.com/GordoTEK
A written version of the TEK is here: https://tinyurl.com/ybl3b8hk
ALWAYS PUT SAFETY FIRST (read the DMT-Nexus Health & Safety Wiki & Stickies):
https://goo.gl/XrE96E
https://goo.gl/H1C1oW
This video is my attempt to share the techniques developed through years of underground research, with an emphasis on safety and best practices. Things that separate this TEK from others - no lab equipment is needed, NO harsh chemicals like sodium hydroxide (LYE) are used, there are no high temperature reactions, no chance for emulsions, no need to measure pH, only grocery store, food grade items are used for the acid and base. Work effort is minimal, yields and purity are high, and it’s easy to do (every step is shown in this video).
Special thanks to Broccoli Samurai and Bass Physics for granting permission to use their music:
http://brocsam.com/
http://www.bassphysics.com/
Thanks DanceSafe.org for the DMT artwork:
https://dancesafe.org/
Thanks MIT for offering FREE online chemistry courses:
https://ocw.mit.edu/courses/chemistry/
It costs you NOTHING to support this work, just click any link below to amazon and I’ll get a small “tip” if you buy anything.
Here is every item you will need for this project:
Cheap round crock pot
https://amzn.to/2MIGO7H
Good value stand mixer
http://amzn.to/2Gbx1DM
The actual stand mixer used in the video
http://amzn.to/2Bnwpaz
Gem Scale (best value)
http://amzn.to/2F9qk3H
Kitchen Scale (great reviews, inexpensive)
http://amzn.to/2BobRP0
Good value blender
http://amzn.to/2Dsq5QR
Actual blender used in video
http://amzn.to/2BoSy8n
Stainless Steel Funnel
https://amzn.to/2HKYhcK
Lens Paper
http://amzn.to/2E2p5E9
Nitrile Gloves
http://amzn.to/2Gc4LAH
Razor Scrapers
http://amzn.to/2E29696
Milligram Measuring Spoons (very helpful to have)
http://amzn.to/2G9smlE
Microscope Slides (optional for solvent evap test)
http://amzn.to/2GiGDMX
[You can get solvent cheaper from a local hardware store, art supply store, or tractor supply, you only need one small can (400ml total)]
Bestine (Heptane)
http://amzn.to/2rBOrWY
VM&P Naphtha
http://amzn.to/2DA8v1q
[You could get the rest from Walmart or a grocery store]
Silicone Spatula
http://amzn.to/2DyqbGJ
Stainless Steel Spoon
http://amzn.to/2DyLVpN
Glass Pie Plates (you need two, this is a two pack)
http://amzn.to/2E2jSw0
Cling Wrap
http://amzn.to/2rDGKzF
Distilled White Vinegar
http://amzn.to/2F7kpfC
Pickling Lime (also search for calcium hydroxide, it can be found on Amazon International sites but should be sold locally for pickling)
http://amzn.to/2E3EmVn
Coffee Filters
http://amzn.to/2G6MG7g
[Finally, the bark -- do your own research here, the first link is to a vendor I trust, with a quality product, ships from the US (this is not an affiliate link)]:
https://u-dont-exist.com/mhrb-powder
Site password is "anatta=no_self" (don't enter the quotes)
[Next is simply a search link, it is NOT an affiliate link and I get nothing for this. The search results may or may not bring up good hits. Always check seller feedback]
https://goo.gl/jjcrXZ
or
https://goo.gl/1BvvQe
Additional notes: While you could let the excess solvent evaporate on its own at room temp, this can take hours and leaves your work subject to contamination from the air, plus you are more likely to accidentally let it completely evaporate which is something you are trying to avoid. Heating these solvents with a warm water bath is standard laboratory procedure (good ventilation is always required). For reference see: https://goo.gl/k4BxjU
If you end up with yellow/brown/reddish colors in your final product, you’ve got plant oil issues. You can add solvent, stir, and then remove and discard the solvent BEFORE adding the lime, this is called “defatting” and it will remove oils without removing any DMT because at that stage the DMT is in its salt form and is not soluble in naphtha or heptane. You can also clean this up after the fact with a recrystalization as described in the video. A defatting step is ALWAYS required with acacia root bark (ACRB).
Also Note: Heptane evaporates MUCH faster than naphtha, so you need to use more for your pulls (150 instead of 100g) reduce the stir time (5 mins instead of 10) and greatly reduce the reduction time, just keep an eye on it, its going to reduce fast. Use good ventilation. Heptane variants are described in the written version of the TEK.