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Don't want to reveal too many details, but I'm trying to figure out if any particular revisions will make a difference with regard to policy actions.  Will it last a day, week, month?  We shall see... next iteration will be a version with zero mention of DMT ;)

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GordoTEK Organic Chemistry Extraction with FAQ (Revised 2019 edition, BEST methods)

If you'd like to support GordoTEK or request a topic, please use patreon, I also post and interact with people there: https://www.patreon.com/GordoTEK A written version of the TEK is here: https://tinyurl.com/ybl3b8hk ALWAYS PUT SAFETY FIRST (read the DMT-Nexus Health & Safety Wiki & Stickies): https://goo.gl/XrE96E https://goo.gl/H1C1oW This video is my attempt to share the techniques developed through years of underground research, with an emphasis on safety and best practices. Things that separate this TEK from others - no lab equipment is needed, NO harsh chemicals like sodium hydroxide (LYE) are used, there are no high temperature reactions, no chance for emulsions, no need to measure pH, only grocery store, food grade items are used for the acid and base. Work effort is minimal, yields and purity are high, and it’s easy to do (every step is shown in this video). Special thanks to Broccoli Samurai and Bass Physics for granting permission to use their music: http://brocsam.com/ http://www.bassphysics.com/ Thanks DanceSafe.org for the DMT artwork: https://dancesafe.org/ Thanks MIT for offering FREE online chemistry courses: https://ocw.mit.edu/courses/chemistry/ It costs you NOTHING to support this work, just click any link below to amazon and I’ll get a small “tip” if you buy anything. Here is every item you will need for this project: Cheap round crock pot https://amzn.to/2MIGO7H Good value stand mixer http://amzn.to/2Gbx1DM The actual stand mixer used in the video http://amzn.to/2Bnwpaz Gem Scale (best value) http://amzn.to/2F9qk3H Kitchen Scale (great reviews, inexpensive) http://amzn.to/2BobRP0 Good value blender http://amzn.to/2Dsq5QR Actual blender used in video http://amzn.to/2BoSy8n Stainless Steel Funnel https://amzn.to/2HKYhcK Lens Paper http://amzn.to/2E2p5E9 Nitrile Gloves http://amzn.to/2Gc4LAH Razor Scrapers http://amzn.to/2E29696 Milligram Measuring Spoons (very helpful to have) http://amzn.to/2G9smlE Microscope Slides (optional for solvent evap test) http://amzn.to/2GiGDMX [You can get solvent cheaper from a local hardware store, art supply store, or tractor supply, you only need one small can (400ml total)] Bestine (Heptane) http://amzn.to/2rBOrWY VM&P Naphtha http://amzn.to/2DA8v1q [You could get the rest from Walmart or a grocery store] Silicone Spatula http://amzn.to/2DyqbGJ Stainless Steel Spoon http://amzn.to/2DyLVpN Glass Pie Plates (you need two, this is a two pack) http://amzn.to/2E2jSw0 Cling Wrap http://amzn.to/2rDGKzF Distilled White Vinegar http://amzn.to/2F7kpfC Pickling Lime (also search for calcium hydroxide, it can be found on Amazon International sites but should be sold locally for pickling) http://amzn.to/2E3EmVn Coffee Filters http://amzn.to/2G6MG7g [Finally, the bark -- do your own research here, the first link is to a vendor I trust, with a quality product, ships from the US (this is not an affiliate link)]: https://u-dont-exist.com/mhrb-powder Site password is "anatta=no_self" (don't enter the quotes) [Next is simply a search link, it is NOT an affiliate link and I get nothing for this. The search results may or may not bring up good hits. Always check seller feedback] https://goo.gl/jjcrXZ or https://goo.gl/1BvvQe Additional notes: While you could let the excess solvent evaporate on its own at room temp, this can take hours and leaves your work subject to contamination from the air, plus you are more likely to accidentally let it completely evaporate which is something you are trying to avoid. Heating these solvents with a warm water bath is standard laboratory procedure (good ventilation is always required). For reference see: https://goo.gl/k4BxjU If you end up with yellow/brown/reddish colors in your final product, you’ve got plant oil issues. You can add solvent, stir, and then remove and discard the solvent BEFORE adding the lime, this is called “defatting” and it will remove oils without removing any DMT because at that stage the DMT is in its salt form and is not soluble in naphtha or heptane. You can also clean this up after the fact with a recrystalization as described in the video. A defatting step is ALWAYS required with acacia root bark (ACRB). Also Note: Heptane evaporates MUCH faster than naphtha, so you need to use more for your pulls (150 instead of 100g) reduce the stir time (5 mins instead of 10) and greatly reduce the reduction time, just keep an eye on it, its going to reduce fast. Use good ventilation. Heptane variants are described in the written version of the TEK.

Comments

Juan

Hi Gordo, please pardon my ignorance. I'd like to ask you about the purpose of the vinegar. I just don't understand why you acidify first just to basify right after. Some other teks just basify. When researching the a/b extraction technique, the acidification is used for pulling some substances and the basification is used for pulling other substances, but in your tek nothing is pulled in between acidification and basification. I only ask because omit the vinegar will reduce the amount of base needed. Is there another purpose for the vinegar in your tek? Thanks in advance.

GordoTEK

This is covered in the FAQ https://www.patreon.com/posts/22774475 under "Q: What is the purpose of the acid in this TEK? or What does the vinegar do that makes you need to put a certain amount and let it sit before you start pulling out the dmt? " A: Yea I didn't explain the chemistry in the video... but what is going on is: In order to separate the DMT from the other compounds in the plant matter (ground bark), the mix has to be chemically modified to make the DMT more ionic and soluble in water. The acid helps make the DMT become more water-soluble and by doing so, helps remove it from the organic layer (the bark material). In other words, the acid converts the DMT to its salt form, and that form will dissolve in the water you added (but will NOT dissolve in naphtha), this helps push the DMT from the plant matter and into the water. But the only way to pull the DMT out of the water is to convert the DMT into its freebase form, which is accomplished by adding the lime (base), after that conversion, the DMT becomes soluble in naphtha, and because of its ionic charge, it is attracted to the solvent and will move into it almost immediately upon contact. This is also why it is OK to add solvent just before adding the base, if you want to remove plant oils, because at this stage, the solvent cannot pull out any DMT, but it will pull out plant fats, so you can safely discard that solvent (and the plant fats that are in it) without concern that you are losing any DMT.

GordoTEK

And yes, I am aware of the numerous straight to base methods (STB), yes it will still work, but I don't think it works as well. The acid/base method is standard organic chem 101 procedure. To read more about A/B extraction see: https://en.wikipedia.org/wiki/Acid-base_extraction

Juan

Thanks for the swift reply. I'm sorry I did not notice the answer in the FAQ. Have a great night.

Bruno

Hi Gordo I have a quick question. After acidifying the bark with vinegar and mixing with water. Instead of just mixing for 40 min could using a ultrasonic bath on a warm setting for those 40 minutes extract more DMT?

GordoTEK

I doubt that it would help much to use an ultrasonic bath but it probably wouldn't hurt either. I have an ultrasonic bath but have not done any experimentation with it specifically for alkaloid extraction, its kind of an interesting thought though.